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2.2 L cleaving agent was formulated in a volume ratio of TFA:H 2 O:EDT= 90:5:5, and pre-frozen for 2 h, and then poured into the 3 L reaction kettle, allowing to react for 2 h at the room temperature
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doi: 10.1172/JCI24422 65 HaeberleHATakizawaRCasolaABrasierARDieterichHJvan RooijenNet al
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