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Figure 3a shows a typical chromatogram with low crude purity due to the formation of various side products involving insertions and deletions of Trp, Phe, Ile/Leu, and Met when the wash-free method was tested with headspace flushing turned off (Table 1, entries 5, 6)
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doi: 10.2337/db06-0080 73 XuEKumarMZhangYJuWObataTZhangNet al
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